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Chem. , 1974,39, 1780; J. Joska, J. Fajkos, and M. , p. 1914. ' 39 The synthetic potential of the Simmons-Smith reaction of trimethylsilyl enol ethers is still being explored. An interesting concentration effect has been noted in the reactions of the cyclic compounds (74; n = 3 or 4), which give the expected cyclopropanol derivatives (75) in dilute solution, but the 2-methylenecycloalkanols (76) in more concentrated solution. It was shown that (76) is formed v i a (75) by a zinc iodidecatalysed rearrangement.

Chem. 96,4075;M. J. S. Dewar and S. , p. 5246; T. Okada, K. Yamaguchi, and T. Fueno, Tetrahedron, 1974, 30, 2293; J. Bertran, V. Forero, F. Mora, and J. I. , 1974,70, 195. B. S. Heller, J. Org. , 197639, 196; E. Fahr, K. Pastille, N. Pel% and D. Scheutzow, Z. , 1974, 29b, 410; F. Nakanishi, H. Nakanishi, Y. Suzuki, M. Hasegawa, and T. Tasai, Japan Kokai, 74 66662 (Chem. , 1974,81, 169309). D. Lenoir and A. Firl, Annalen, 1974, 1467. B. L. Adams and P. Kovacic, J . Amer. Chem. , 1974,%, 7014. B.

Sci. chim.. 1974, 22,467 (Chem. , 1974, 81, 151900). 'I8 ''O "' "' 123 lZ4 H. Hart and M. Nitta, Tetrahedron Letters, 1974, 2109, 2113. M. Sato, S. Ebine, and J. S. , 1974, 846. R. Barlet, Compt. , 1974, 278, C , 621 ; P. A. Verbrugge and E. W. Urbanus, Ger. , 2324390 (Chem. , 1974, SO, 70420. C . B. Chapleo, C. B. Dahl, A. S. Dreiding, R. Grieb, and A. Niggli, Helo. Chim. , 1974, 57, 1876. Y. M. Sheikh, J. Leclercq, and C. S. Perkin I , 1974, 909. R. Mathias and P. Weyerstahl, Angew. Chem Internat.

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